| Board of Editors |
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xxi | |
| Chronology of Organic Reactions Catalysis Society Conferences |
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xxiii | |
| Preface |
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xxv | |
| I. Symposium on Catalysis in Organic Synthesis |
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1 | |
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1. On the Use of Immobilized Metal Complex Catalysts in Organic Synthesis |
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3 | |
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Christopher W. Jones,¹,² Michael Holbach,² John Richardson,¹ William Sommer,² Marcus Weck,² Kunquan Yu,¹ and Xiaolai Zheng¹,² |
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¹Georgia Institute of Technology, School of Chemical & Biomolecular Engineering and ²School of Chemistry and Biochemistry, Atlanta, GA 30332 |
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2. Supported Re Catalysts for Metathesis of Functionalized Olefins |
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13 | |
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Anthony W. Moses, Heather D. Leifeste, Naseem A. Ramsahye, Juergen Eckert and Susannah L. Scott |
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Department of Chemical Engineering, University of California, Santa Barbara CA 93106-5080 |
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3. Catalytic Hydrogenation of a Schiff's Base over Pd/Carbon Catalysts: Kinetic Prediction of Impurity Fate and Byproduct Formation |
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23 | |
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Steve S.Y.Wang, William F. Merkl, Hyei-Jha Chung, Wendel Doubleday and San Kiang |
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Process Research and Development, Bristol-Myers Squibb Company, One Squibb Drive, New Brunswick, NJ 08903-0191 |
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4. Halophosphite Ligands for the Rhodium Catalyzed Low-Pressure Hydroformylation Reaction |
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31 | |
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Eastman Chemical Company, Texas Eastman Division, P.O. Box 7444, Longview TX 75607-7444 |
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5. Development of a Monolithic Bioreactor: Tailor-Made Functionalized Carriers |
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39 | |
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Karen M. de Lathouder, Freek Kapteijn and Jacob A. Moulijn |
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Delft University of Technology, Faculty of Applied Sciences, DelftChemTech, Section R&CE, Julianalaan 136, 2628 BL Delft, The Netherlands |
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6. Highly Selective Preparation of trans-4-Aminocyclohexane Carboxylic Acid from cis-Isomer over Raney® Nickel Catalyst |
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45 | |
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Sándor Göbölös, Zoltán Banka, Zoltán Tóth, János Szammer, and József L. Margitfalvi |
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Chemical Research Center, Institute of Surface Chemistry and Catalysis, 1025 Budapest, Pusztaszeri ut 59-67, Hungary |
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7. Gas-Phase Acetone Condensation over Hydrotalcite-like Catalysts |
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55 | |
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Francisco Tzompantzi¹, Jaime S. Valente², Manuel S. Cantú² and Ricardo Gómez¹,² |
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¹Universidad Autónoma Metropolitana-Iztapalapa, San Rafael Atlixco No 152, México 09340, D.F. |
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²Instituto Mexicano del Petróleo, Eje Central Lazaro Cardenas #152, México, D.F. 07730. |
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8. Gas Phase Trimerization of Isobutene Using Green Catalysts |
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61 | |
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Angeles Mantilla,¹ Francisco Tzompantzi,² Miguel Torres¹ and Ricardo Gómez² |
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¹Universidad Autónoma Metropolitana Azcapotzalco. Av. San Pablo 180, Reynosa Tamaulipas, Azcapotzalco, México, 02200, D.F. |
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²Universidad Autónoma Metropolitana, Iztapalapa, Depto. de Quimica, Av. San Rafael Atlixco 152, México 09340 D.F. |
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9. Synthesis of Methyl Isobutyl Ketone over a Multifunctional Heterogeneous Catalyst: Effect of Metal and Base Components on Selectivity and Activity |
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67 | |
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Arran S. Canning, Jonathan J. Gamman, S. David Jackson and Strath Urquart |
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WestCHEM, Dept. of Chemistry, The University, Glasgow G12 8QQ, Scotland, UK. |
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10. The Control of Regio- and Chemo-Selectivity in the Gas-phase, Acid-Catalyzed Methylation of 1,2-Diphenol (Catechol) |
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77 | |
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Mattia Ardizzi, Nicola Ballarini, Fabrizio Cavani, Luca Dal Pozzo, Luca Maselli, Tiziana Monti and Sara Rovinetti |
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University of Bologna, Dipartimento di Chimica Industriale e dei Materiali, Viale Risorgimento 4, 40136 Bologna, Italy. |
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11. The Environmentally Benign, Liquid-phase Benzoylation of Phenol Catalyzed by H-β Zeolite. An Analysis of the Reaction Scheme. |
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83 | |
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Mattia Ardizzi, Nicola Ballarini, Fabrizio Cavani, Massimo Cimini, Luca Dal Pozzo, Patrizia Mangifesta and Diana Scagliarini |
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University of Bologna, Dipartimento di Chimica Industriale e dei Materiali, Viale Risorgimento 4, 40136 Bologna, Italy. |
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| II. Symposium on Catalytic Oxidation |
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89 | |
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12. Biphasic Catalytic Oxidation of Hydrocarbons Using Immobilized Homogeneous Catalyst in a Microchannel Reactor |
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91 | |
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Jianli Hu, Guanguang Xia, James F. White, Thomas H. Peterson and Yong Wang |
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Pacific Northwest National Laboratory, 902 Battelle Boulevard, Richland, WA 99352 |
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13. Reaction Pathways for Propylene Partial Oxidation on Au/TiO2 |
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99 | |
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Rahul Singh and Steven S.C. Chuang |
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Department of Chemical and Biomolecular Engineering, University of Akron, Akron OH, 44325-3906 |
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14. The Transformation of Light Alkanes to Chemicals: Mechanistic Aspects of the Gas-phase Oxidation of n-Pentane to Maleic Anhydride and Phthalic Anhydride |
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109 | |
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Mirko Bacchini¹, Nicola Ballarini¹, Fabrizio Cavani¹, Carlotta Corte Stefano Cortesi¹, Carlo Fumagalli², Gianluca Mazzoni², Tiziana Monti², Francesca Pierelli¹, Ferruccio Trifirò¹¹ |
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¹Dipartimento di Chimica Industriale e dei Materiali, Viale Risorgimento 4, 40136 Bologna, Italy. INSTM, Research Unit of Bologna A member of the Concorde CA and Idecat NoE (6FP of the EU). |
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²Lonza SpA, Via E. Fermi 51, 24020 Scanzorosciate (BG), Italy |
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15. Transition Metal Free Catalytic Aerobic Oxidation of Alcohols Under Mild Conditions Using Stable Nitroxyl Free Radicals |
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119 | |
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Setrak K. Tanielyan¹, Robert L. Augustine¹ , Clementina Reyes¹, Nagendranath Mahata¹, Michael Korell² and Oliver Meyer³ |
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¹Center for Applied Catalysis, Seton Hall University, South Orange, NJ 07079 |
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²DegussaCorp. BU Building Blocks, Parsippany, NJ 07054 |
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³Degussa AG, BU Building Blocks, Marl 45764 Germany |
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16. The Conversion of Aminoalcohols to Aminocarboxylic Acid Salts over ChromiaPromoted Skeletal Copper Catalysts |
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131 | |
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Dongsheng S. Liu, Noel W. Cant and Andrew J. Smith |
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School of Chemical Engineering and Industrial Chemistry, The University of New South Wales, Sydney, NSW 2052, Australia |
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17. Bromine-Free TEMPO-Based Catalyst System for the Oxidation of Primary and Secondary Alcohols Using NaOCl as the Oxidant |
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141 | |
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Setrak K. Tanielyan¹, Robert L. Augustine¹, Indra Prakash², Kenneth E. Furlong² and Handley E. Jackson² |
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¹Center for Applied Catalysis, Seton Hall University, South Orange, NJ 07079 |
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²The NutraSweet Corporation, Chicago, IL 60654 |
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18. In situ Infrared Study of Catalytic Oxidation over Au/TiO2 Catalysts |
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147 | |
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Duane D. Miller and Steven S.C. Chuang |
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Dept. of Chemical and Biomolecular Engineering, University of Akron, Akron, OH 44325-3906, USA |
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| III. Symposium on Catalytic Hydrogenation |
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153 | |
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19. 2006 Murray Raney Award Lecture: Synthesis and Features of New Raney® Catalysts from Metastable Precursors |
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155 | |
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Osaka University, Yamadaoka 2-1 Suita, Osaka, 565-0871 Japan |
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20. Competitive Hydrogenation of Nitrobenzene, Nitrosobenzene and Azobenzene |
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167 | |
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Elaine A. Gelder', S. David Jackson¹, C. Martin Lok² |
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¹WestCHEM, Department of Chemistry, The University, Glasgow, G12 8QQ Scotland |
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²Johnson Matthey Catalysts, Belasis Avenue, Billingham, Cleveland, TS23 1LB U.K. |
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21. Selective Hydrogenation of Dehydrolinalool to Linalool Using Nanostructured Pd-Polymeric Composite Catalysts |
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177 | |
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Linda Z. Nikoshvilia , Ester M. Sulmana , Galine N. Demidenkoa, Valentina G. Matveevaa , Mikhail G. Sulmana, Ludmila M. Bronsteinb Petr M. Valetskiyc and Irina B. Tsvetkovaa |
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a Dept. of Biotechnology and Chemistry, Tver Technical University, A. Nikitina str., 22, 170026, Tver, Russia |
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b Chemistry Department, Indiana University, Bloomington, IN 47405, USA Wesmeyanov Institute of Organoelement Compounds of RAS, Vavilov str., 28, Moscow, Russia |
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22. Modeling and Optimization of Complex Three-Phase Hydrogenations and Isomerizations under Mass-Transfer Limitation and Catalyst Deactivation |
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187 | |
|
Tapio O. Salmi, Dmitry Yu. Murzin, Johan P. Wärnå, Jyri-Pekka Mikkola, Jeanette E.B. Aumo, and Jyrki I. Kuusisto |
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Åbo Akademi, Process Chemistry Centre, FI-20500 Turku/Åbo, Finland |
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23. The Effects of Various Catalyst Modifiers on the Hydrogenation of Fructose to Sorbitol and Mannitol |
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197 | |
|
Daniel J. Ostgard, Virginie Duprez, Monika Berweiler, Stefan Röder and Thomas Tacke |
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Degussa AG, Rodenbacher Chaussee 4, 63457 Hanau, Germany |
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24. Cavitating Ultrasound Hydrogenation of Water-Soluble Olefins Employing Inert Dopants: Studies of Activity, Selectivity and Reaction Mechanisms |
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213 | |
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Robert S. Disselkamp, Sarah M. Chajkowski, Kelly R. Boyles, Todd R. Hart, Charles H.F. Peden |
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Institute for Interfacial Catalysis, Pacific Northwest National Laboratory, Richland, WA 99352 USA |
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25. The Treatment of Activated Nickel Catalysts for the Selective Hydrogenation of Pynitrile |
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227 | |
|
Daniel J. Ostgard¹, Felix Roessler, Reinhard Karge² and Thomas Tacke¹ |
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¹Degussa AG, Exclusive Synthesis and Catalysts, Rodenbacher Chaussee 4, D-63457 Hanau, Germany |
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²DSM Nutritional Products Ltd, Postfach 3255, CH-4002 Basel, Switzerland |
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26. Deactivation of Sponge Nickel and Ru/C Catalysts in Lactose and Xylose Hydrogenations |
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235 | |
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Jyrki Kuusisto, Jyri-Pekka Mikkola and Tapio Salmi |
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Laboratory of Industrial Chemistry, Process Chemistry Centre, Åbo Akademi University, Biskopsgatan 8, FIN-20500 Turku, Finland |
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27. Selectivity Control in 1-Phenyl-1-Propyne Hydrogenation: Effect of Modifiers |
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241 | |
|
S. David Jackson and Ron R. Spence |
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WestCHEM, Department of Chemistry, The University, Glasgow, G12 8QQ, Scotland |
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28. Hydrogenation and Isomerization Reactions of Olefinic Alcohols Catalyzed in Homogeneous Phase by Rh(I) Complexes |
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247 | |
|
Maria G. Musolino, Giuseppe Apa, Andrea Donato and Rosario Pietropaolo |
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Department of Mechanics and Materials, Faculty of Engineering, University of Reggio Calabria, Loc. Feo di Vito, 1-89060 Reggio Calabria, Italy |
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29. Reductive Amination of Isobutanol to Diisobutylamine on Vanadium Modified Raney® Nickel Catalyst |
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253 | |
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Sándor Gobölös and József L. Margitfalvi |
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Chemical Research Center, Institute of Surface Chemistry and Catalysis, H-1025 Budapest, Pusztaszeri zit 59-67, Hungary |
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| IV. Symposium on Novel Methods in Catalysis of Organic Reactions |
|
259 | |
|
30. How to Find the Best Homogeneous Catalyst |
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261 | |
|
Gadi Rothenberg¹, Jos A. Hageman², Frederic Clerc³, Hans-Werner Frühauf¹ and Johan A. Westerhuis² |
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¹Van't Hoff Institute for Molecular Sciences and ²Swammerdam Institute of Life Sciences, University of Amsterdam, Nieuwe Achtergracht 166, 1018 WV Amsterdam, The Netherlands. ³Institut de Recherches sur la Catalyse, 2 avenue Albert Einstein, 69626 Villeurbanne Cedex, France |
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31. Novel Chloroaluminate Ionic Liquids for Arene Carbonylation |
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271 | |
|
Ernesto J. Angueira and Mark G. White |
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School of Chemical and Biomolecular Engineering, Georgia Institute of Technology, Atlanta, GA 30332-0100 |
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32. Chemoselective Hydrogenation of Nitro Compounds to the Corresponding Amines on Raney® Copper Catalysts |
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281 | |
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Simon Robitaille, Genevieve Clément, Jean Marc Chapuzet and Jean Lessard |
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Laboratoire de Chimie et Electrochimie Organiques, Département de Chimie, Université de Sherbrooke, Sherbrooke, Québec J1K 2R1, Canada |
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33. Selective Hydrogenolysis of Sugar Alcohols over Structured Catalysts |
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289 | |
|
Chunshe (James) Cao, James F. White, Yong Wang and John G. Frye |
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Pacific Northwest National Laboratory |
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902 Battelle Blvd, MS K8-93, Richland, WA 99352 |
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34. Twinphos: A New Family of Chiral Ferrocene Tetra-Phosphine Ligands for Asymmetric Catalytic Transformations |
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293 | |
|
Benoit Pugin, Heidi Landert, Martin Kesselgruber, Hans Meier, Richard Sachleben, Felix Spindler and Marc Thommen |
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Solvias AG, Klybeckstrasse 19, Postfach CH 4002, Basel, Switzerland |
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35. Catalyst Library Design for Fine Chemistry Applications |
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303 | |
|
József L. Margitfalvi, András Tompos, Sándor Gobölös, Emila Tálas and Mihály Hegedus |
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Chemical Research Center, Institute of Surface Chemistry and Catalysis, Department of Organic Catalysis, 1025 Budapest, Pusztaszeri ut 59-67Hungary |
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36. Dendrimer Templates for Pt and Au Catalysts |
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315 | |
|
Bethany J. Auten, Christina J. Crump, Anil R. Singh and Bert D. Chandler Department of Chemistry, Trinity University, 1 Trinity Place, San Antonio, TX 78212-7200 |
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| V. Symposium on Acid and Base Catalysis |
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325 | |
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37. Development of an Industrial Process for the Lewis Acid/Iodide Salt-Catalyzed Rearrangement of 3,4-Epoxy-l-Butene to 2,5-Dihydrofuran |
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327 | |
|
Stephen N. Falling¹, John R. Monnier,¹,² Gerald W. Phillips¹, Jeffrey S. Kanel¹, and Stephen A. Godleski³ |
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¹Eastman Chemical Company Research Laboratories, Bldg. 150B, P.O. Box 1972 Kingsport, TN 37662-5150 |
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²Department of Chemical Engineering, University of South Carolina, Columbia, SC, 29208 |
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³Eastman Kodak Company, Rochester, New York, 14650 |
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38. A New Economical and Environmentally Friendly Synthesis of 2,5-Dimethyl-2,4-Hexadiene |
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337 | |
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Alessandra O. Bianchia, Valerio Borzattaa, Elisa Poluzzia and Angelo Vaccarib |
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a Endura SpA, Viale Pietramellara 5, 40012 Bologna (Italy) |
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b Dipartimento di Chiinica Industriale e dei Materials, Alma Mater Studiorum University di Bologna, Viale del Risorgimento 4, 40136 Bologna, Italy |
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39. Supported Heteropoly Acid Catalysts for Friedel-Crafts Acylation |
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347 | |
|
Kenneth G. Griffin¹, Peter Johnston¹, Roger Prétôt², Paul A. van der Schaaf² |
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¹Johnson Matthey plc, Catalyst Development, Royston, SG8 5HE, UK |
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²Ciba Specialty Chemicals Inc., CH-4002 Basel, Switzerland |
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40. Synthesis of Pseudoionones by Aldol Condensation of Citral with Acetone on Li-Modified MgO Catalysts |
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355 | |
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Veronica K. Diez, Juana Di Cosimo and Carlos Apesteguia |
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Catalysis Science and Engineering Research Group (GICIC), Institute de Investigaciones en Catalisis y Petroquimica (UNL-CONICET), Santiago del Estero 2654(3000) Santa Fe, Argentina |
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41. The One Step Synthesis of MIBK via Catalytic Distillation: A Preliminary Pilot Scale Study |
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365 | |
|
William K. O'Keefe, Ming Jiang, Flora T.T. Ng and Garry L. Rempel |
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The University of Waterloo, Department of Chemical Engineering, 200 University Avenue West, Waterloo, Ontario, Canada N2L 3G1 |
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| VI. Symposium on "Green" Catalysis |
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375 | |
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42. Producing Polyurethane Foam from Natural Oil |
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377 | |
|
Aaron Sanders, David Babb, Robbyn Prange, Mark Sonnenschein, Van Delk, Chris Derstine and Kurt Olson |
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The Dow Chemical Company, 2301 N Brazosport Blvd., Freeport, TX 77541 |
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43. Carbonylation of Chloropinacolone: A Greener Path to Commercially Useful Methyl Pivaloylacetate |
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385 | |
|
Joseph R. Zoeller and Theresa Barnette |
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Eastman Chemical Company, P.O. Box 1972, Kingsport, TN 37662 |
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44. Recycling Homogeneous Catalysts for Sustainable Technology |
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395 | |
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Jason P. Hallett, Pamela Pollet, Charles A. Eckert and Charles L. Liotta |
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School of Chemistry and Biochemistry, School of Chemical & Biomolecular Engineering, and Specialty Separations Center, Georgia Institute of Technology, Atlanta, Georgia 30332-0325 |
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45. "Green" Catalysts for Enhanced Biodiesel Technology |
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405 | |
|
Anton A. Kiss, Gadi Rothenberg and Alexandre C. Dimian |
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University of Amsterdam, van 't Hoff Institute for Molecular Sciences, Nieuwe Achtergracht 166, 1018 WV Amsterdam, The Netherlands |
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46. Continuous Deoxygenation of Ethyl Stearate: A Model Reaction for Production of Diesel Fuel Hydrocarbons |
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415 | |
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Mathias Snåre, Iva Kubicková, Päivi Mäki-Arvela, Kari Eränen and Dmitry Yu. Murzin |
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Laboratory of Industrial Chemistry, Process Chemistry Centre, Åbo Akademi University Biskopsgatan 8, FIN-20500 Turku/Åbo, Finland |
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47. Glycerol Hydrogenolysis to Propylene Glycol under Heterogeneous Conditions |
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427 | |
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Simona Marincean, Lars Peereboom, Yaoyan Xi, Dennis J. Miller and James E. Jackson |
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Department of Chemistry, Department of Chemical Engineering and Materials Science, Michigan State University, East Lansing MI 48824-1322 |
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48. Developing Sustainable Process Technology |
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437 | |
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UOP LLC, 25 East Algonquin Road, Des Plaines, IL 60017-5017 |
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49. Selective Oxidation of Propylene to Propylene Oxide in CO2 Expanded Liquid System |
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447 | |
|
Hyun-Jin Lee, Tie-Pan Shi, Bala Subramaniam and Daryle H. Busch |
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Center for Environmentally Beneficial Catalysis, University of Kansas, Lawrence, KS 66047 |
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| VII. Symposium on Other Topics in Catalysis |
|
453 | |
|
50. catASium® M: A New Family of Chiral Bisphospholanes and their Application in Enantioselective Hydrogenations |
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455 | |
|
Thomas H. Riermeier,(a) Axel Monsees,a Jens Holz,(b) Armin Börner(b) and John Tarabocchia(c) |
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a Degussa AG, Degussa Homogeneous Catalysts, Rodenbacher Chaussee 4, 63457 Hanau-Wolfgang, Germany |
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b Leibniz-Institut for Organische Katalyse an der Universitdt Rostock e. V., Buchbinderstr. 5/6, 18055 Rostock, Germany |
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c Degussa Corporation, 379 Interpace Parkway, Parsippany, NJ 07054 |
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51. Synthesis of Chiral 2-Amino-1-Phenylethanol |
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463 | |
|
Robert Augustine, Setrak Tanielyan, Norman Marin and Gabriela Alvez |
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Center for Applied Catalysis, Seton Hall University, South Orange, NJ 07079 |
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52. Selective Tertiary-Butanol Dehydration to lsobutylene via Reactive Distillation and Solid Acid Catalysis |
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469 | |
|
John F. Knifton(a) and John R. Sanderson(b) |
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a Consultant; P.O. Box 200333, Austin, TX 78720 |
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53. Leaching Resistance of Precious Metal Powder Catalysts - Part 2 |
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475 | |
|
Tim Pohlmann, Kimberly Humphries, Jaime Morrow, Tracy Dunn, Marisa Cruz, Konrad Möbus and Baoshu Chen |
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Degussa Corporation, 5150 Gilbertsville Highway, Calvert City, KY 42029 |
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54. Optimization of Reductive Alkylation Catalysts by Experimental Design |
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481 | |
|
Venu Arunajatesan, Marisa Cruz, Konrad Möbus and Baoshu Chen |
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Degussa Corporation, 5150 Gilbertsville Hwy, Calvert City, KY 42029 |
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55. Accelerated Identification of the Preferred Precious Metal Powder Catalysts for Selective Hydrogenation of Multi-functional Substrates |
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487 | |
|
Dorit Wolf, Steffen Seebald and Thomas Tacke |
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|
Degussa AG, Exclusive Synthesis & Catalysts, EC-KA-RD-WG Rodenbacher Chaussee4 D-63457 Hanau (Wolfgang), Germany |
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56. Transition Metal Removal from Organic Media by Deloxan® Metal Scavengers |
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493 | |
|
Jaime B. Woods¹, Robin Spears¹, Jurgen Krauter², Tim McCarthy³, Micheal Murphy³, Lee Hord4, Peter Doorley4 and Baoshu Chen¹ |
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¹Degussa Corporation, Business Line Catalysts, 5150 Gilbertsville Hwy., Calvert City, KY 42029; |
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²Degussa AG, Business Line Catalysts, Rodenbacher Chaussee 4, D-63457, Hanau, Germany; |
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³Degussa Corporation, Business Line Catalysts, 379 Interpace Parkway, Parsippany, NJ, 07054; |
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4Mobile Process Technology, 2070 Airways Boulevard, Memphis, TN, 38114 |
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57. Electroreductive Pd-Catalyzed Ullmann Reactions in Ionic Liquids |
|
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501 | |
|
Laura Durán Pachón and Gadi Rothenberg |
|
|
|
Van 't Hoff Institute for Molecular Sciences, University of Amsterdam, Nieuwe Achtergracht 166, 1018 WV Amsterdam, The Netherlands |
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|
| Author Index |
|
507 | |
| Keyword Index |
|
513 | |
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