More Modern Chemical Techniques

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Format: Paperback
Pub. Date: 2002-02-01
Publisher(s): Royal Society of Chemistry
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Summary

Analytical techniques are powerful tools in a chemist's armoury. Spectroscopic data and chemical information are used routinely in laboratories to follow a chemical reaction or elucidate a chemical structure. However, the sophistication of the analytical techniques used changes rapidly, hence the routinely used method of today can all too readily be superseded by the new technology of tomorrow. More Modern Chemical Techniques identifies some applications of the important chemical techniques in use today that are less well known in schools and colleges and which illustrate how chemistry is using state -of-the-art technology to push back the frontiers of the subject. Examples include: elemental analysis such as atomic absorption spectrometry and inductively coupled plasma techniques; separations including electrophoresis, structure determination (eg x-ray diffraction and optical microscopy); and sampling and sample preparation.

Table of Contents

Introduction
Acknowledgements
Elemental analysisp. 1
Atomic absorption spectrometry (AAS)p. 1
Flame atomic absorption spectrometry (FAAS)p. 8
Graphite furnace atomic absorption spectrometry (GFAAS)p. 15
Hydride generation atomic absorption spectrometry (HGAAS)p. 17
Cold vapour atomic absorption spectrometry (CVAAS)p. 19
Inductively coupled plasma (ICP) techniquesp. 25
Inductively coupled plasma-atomic emission spectrometry (ICP-AES)p. 25
Inductively coupled plasma-mass spectrometry (ICP-MS)p. 34
X-ray fluorescence spectrometry (XRF)p. 43
Energy dispersive XRF (EDXRF)p. 54
Elemental microanalysisp. 61
Separationsp. 73
Gel electrophoresisp. 73
Capillary electrophoresisp. 109
Structuresp. 131
X-ray crystallographyp. 131
Powder X-ray diffraction (PXD)p. 153
Optical microscopyp. 157
Sampling and sample preparationp. 169
Bibliographyp. 184
Table of Contents provided by Blackwell. All Rights Reserved.

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